Home | Legals | Sitemap | KIT
Arndt Last
Dr. Arndt Last
Polymer X-ray lenses for beam shaping and X-ray microscopy

Phone: +49 721 608-23817
arndt lastNbd5∂kit edu

Staff webpage

Pascal Meyer
Dr. Pascal Meyer
Grating based interferometry

Phone: +49 721 608-23924
pascal meyerNdl8∂kit edu

Staff webpage

Danays Kunka
Dr. Danays Kunka
Emerging X-ray optics

Phone: +49 721 608-23864
danays kunkaFrd5∂kit edu

Staff webpage

Research Area
Collaborations

More…

External link
x-ray-optics.de

x-ray-optics.de

X-ray Optics

Dr. Danays Kunka | Dr. Arndt Last | Dr. Pascal Meyer

We are developing new X-ray optical components which are used to improve existing or to establish new X-ray imaging techniques. The components are made either from X-ray stable polymer or metal and are fabricated using lithography methods (X-ray, E-Beam, laser and optical lithography) and subsequent electroforming available through KNMF. New imaging modalities are developed together with different collaboration partners. The R&D activities are divided in three main parts:
 

Polymer X-ray lenses for beam shaping and X-ray microscopy

Under this topic we are developing and fabricating Compound Refractive X-ray Lenses (CRL) which are used for sample illumination with focal spot size down to 100 nm and to build up full field X-ray microscopes. X-ray Prism Lenses (XPL) are realized for shaping the X-ray beams and for homogenous sample illumination. All activities are application oriented. Although the main focus is on synchrotron use, we also target for applications at X-ray tubes and at X-FELs.

Read more…

The refractive index n for X-rays with photon energies of 10 keV – 50 keV is in the range of n = 1- Δn = 1 - 10-5 to 1 - 10-7 resulting in a small refractive power of the lens material. As n is below one, the lens elements of a focusing lens have to be biconcave, in contrary to lenses for visible light. In the case of X-rays, short focal lengths can only be achieved by positioning a large number of strongly curved lenses in a row. Using deep X-ray lithography available through KNMF, rows of such lens structures are fabricated in X-ray-stable polymer (for energies in the range of 8 – 50 keV) or in nickel (for 50 – 500 keV) on substrates in one step without time-consuming individual-lens alignment. Line focus lenses are fabricated within one exposure step. Point focus lenses are obtained by combining two line focus lenses tilted by 90° around the optical axis.

Microscopy resolutions below 200 nm (line and space) in a field of view of 70 µm x 70 µm have been obtained so far by means of IMT CRLs. The apertures of parabolic lenses are in the range of 50 µm up to 1.5 mm. The focal distances can be in the few centimeters range. XPLs illumination optics are made with apertures of up to 1.5 mm and prism sizes down to 15 µm. Special beam shaping optics have been realized to transform for example a narrow 1 mm X-ray beam with Gaussian intensity distribution from a high brilliance synchrotron source into a wide 6 mm beam with a top-hat intensity distribution. In this way larger samples can be imaged.

Current research activities are dedicated to

  • Improving resolution and increasing the field of view in full field microscopy
  • Developing X-ray microscopes with optimized condenser and objectives
  • Demonstrate the use of the X-ray lenses at X-ray tubes
  • Development of low absorption, large aperture prism or mosaic optics
  • Optimization of beam shaping optics
  • Development of CRLs with variable focal length


Schematic view of an X-ray full field microscope

 

   
Parabolic line focus lens   Point focus lens   X-ray prism lens

 

Grating based interferometry

Grating based interferometry relies strongly on high quality, high aspect ratio X-ray gratings. With our activities we are following the four demanding requests for high performance gratings which need to be fulfilled to bring this imaging technique to commercial application in medical diagnostics and materials analysis: larger (in terms of the grating area), higher (in view of structural height), better (in terms of quality and homogeneity) and smaller (in terms of grating periods). This needs process development, process modification, structural characterization and understanding of effects arising during processing.

Read more…

     
A 10 µm period gratings with sun-rays (before electroplating)    

X-ray LIGA KIT logo in gold in front of a grating (courtesy of JulesMarketing).

We continuously improve the gratings quality with focus on the following issues :

  • reproducibility of the process,
  • downsizing the period and increasing the resist/metal thickness by modifying the photoresist sensitivity and contrast,
  • increasing the mechanical stability by finding the best combination of applied dose and post exposure bake (PEB), by using freeze drying and room temperature electroplating,
  • minimizing the harmful effects of secondary radiation by using a low Z electroplating layer/substrate, optimizing the design and the gratings’ geometry to obtain the minimum possible deviation from an ideal binary grating,

The characterization is done using:

  • scanning electron microscopy (DC measurement),
  • white light interferometry (G1 measurement thickness)
  • visibility measurement using standard grating setups by our partners (CT-Lab, TUM, FAU).

 

Emerging X-ray optics

For broadening the X-ray imaging modalities for biomedical and material science applications at synchrotron facilities and at X-ray laboratories novel optical elements with two- and three dimensions are developed. They are used for multi-modal information acquisition based on small angle scattering, absorption and phase contrast.

Read more…

The current activities concentrate on process and methodology development to pattern and characterize two-dimensional gratings for investigation of dynamical processes. Furthermore, considerable research is devoted to enhance the synthesis of the polymer used in the lithography process to obtain better physical-chemical properties and to use the optimized formulation in the fabrication of HAR grating structures. The novel structures will be employed as the main optical elements in Grating-based interferometry and Single-Shot imaging modalities to investigate weak X-ray absorbing samples and composite material with similar absorption cross-sections by phase and dark field Imaging.

Teaching, Education, Jobs

We are member of the Karlsruhe School of Optics and photonics KSOP and train students in X-ray optics and imaging by offering.

  • Seminar courses
  • Lab courses
  • Internships

We are also offering research topics for bachelor and master thesis to students from all over the world.

Arndt Last gives lectures at the Department of Mechanical Engineering under the topic:

X-ray Optics (WS / SS)

Usually 6 to 8 Ph.D. students are doing their Ph.D. work in the group. Open positons will be advertised on KIT’s website for job offers.

 

NEWS

Japanese publications based on KIT/IMT X-ray lenses
225 Japanese publications based on KIT/IMT X-ray lenses

In the last 10 years, from 2008 to 2017, at the synchrotron source SPring-8 in Japan 225 publications have been published where compound refractive X-ray lenses (CRLs) from KIT/IMT have been used in the experimental setup. This makes a total of nearly 1500 pages published by scientists at the beamlines BL10XU, BL13XU, BL15XU, BL22XU, BL24XU, BL41XU and BL43LXU. All these papers are based on measurements where CRLs from IMT helped illuminating the sample in diverse experimental methods like for example micro diffraction, resonant scattering, micro-XAFS, GISAXS or ultra-high pressure research.

Refractive x-ray lenses from KIT/IMT.
IMT’s compound refractive X-ray lenses in user operation at ESRF, ID01

ESRF announced that the Full Field Diffraction X-ray Microscopy (FFDXM) end station at the ID01 is now open to user experiments. This new method uses X-ray lenses from KIT/IMT specially designed for the imaging part of the setup.

 
X-ray beam shaping by polymer lenses
IMT’s beam shaping X-ray optics awarded at XRM 2016

Ottó Márkus, Ph.D. student in the X-ray optics group, was awarded with the best poster price at the X-ray microscopy conference XRM 2016 for his poster entitled “X-ray beam shaping by polymer lenses”.